Mercury is quantitatively retained with 1, 5-diphenylcarbazone (DPC) on microcrystalline naphthalene in the pH range 6.5-8.5 from a large volume of aqueous solutions of various samples. After filtration, the solid mass consisting of the mercury complex and naphthalene was dissolved in 5.0 mL of dimethylformamide (DMF) and mercury was determined by spectrophotometric method at 542 nm against the reagent blank. The linear calibration range for mercury was 30-1800 1.tg L-1 in DMF solution with a detection limit of 20 lug L-1. The relative standard deviation for eight replicate measurements of 1.0 [ig of mercury in 5.0 mL of DMF was 2.5%. The effect of potential interfering ions was investigated and the proposed method was applied to the determination of mercury in water samples.
Shishehbore, M. R., Nasirizadeh, N., & Akhoundi, A. M. (2008). Spectrophotometric Determination of Hg2+ after Solid Phase Extraction on Microcrystalline Naphthalene. Journal of Physical & Theoretical Chemistry, 5(2), 29-34.
MLA
M. Reza Shishehbore; Navid Nasirizadeh; A. Mohammad Akhoundi. "Spectrophotometric Determination of Hg2+ after Solid Phase Extraction on Microcrystalline Naphthalene". Journal of Physical & Theoretical Chemistry, 5, 2, 2008, 29-34.
HARVARD
Shishehbore, M. R., Nasirizadeh, N., Akhoundi, A. M. (2008). 'Spectrophotometric Determination of Hg2+ after Solid Phase Extraction on Microcrystalline Naphthalene', Journal of Physical & Theoretical Chemistry, 5(2), pp. 29-34.
VANCOUVER
Shishehbore, M. R., Nasirizadeh, N., Akhoundi, A. M. Spectrophotometric Determination of Hg2+ after Solid Phase Extraction on Microcrystalline Naphthalene. Journal of Physical & Theoretical Chemistry, 2008; 5(2): 29-34.